ISO 1693:1976

Cryolite, natural and artificial — Determination of fluorine content — Modified Willard-Winter method

OVERVIEW

Specifies the determination for natural and synthetic materials having a molar ratio sodium fluoride/aluminium trifluoride between 3 and 1,7 approximately. The principle consists in fusion of a test portion with sodium carbonate, separation of fluorine by distillation with sulphuric acid or perchloric acid. Titration with thorium nitrate solution in presence of sodium alizarinsulphonate/methylene blue as indicator. Alternatively, the thorium nitrate titration may be made using only sodium alizarinsulphonate, the end-point being*spectrophotometrically determined at 525 nm.

COMMENTS

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PRODUCT DETAILS

Status Current
Edition 1976
No. of Pages 6
ICS Classification 71.060.50 Salts
Committee ISO/TC 226
Available for Purchase For sale in Singapore only
Adoption ISO